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ChemicalBook CAS DataBase List (S)-(+)-5-METHYL-1-HEPTANOL

(S)-(+)-5-METHYL-1-HEPTANOL synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: Mg / diethyl ether
1.2: CuI / -50 - 20 °C
2.1: BH3 / tetrahydrofuran / 5 h / 20 °C
2.2: 2.7 g / 1 M aq. NaOH; 35 percent H2O2 / tetrahydrofuran / 2 h / 20 °C

References:

Tai, Akira;Syouno, Emi;Tanaka, Kazuki;Fujita, Morifumi;Sugimura, Takashi;Higashiura, Yasutomo;Kakizaki, Masashi;Hara, Hideho;Naito, Tikahiko [Bulletin of the Chemical Society of Japan,2002,vol. 75,# 1,p. 111 - 121]

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