ChemicalBook CAS DataBase List Sinitrodil

Sinitrodil synthesis

5synthesis methods

Product Name:Sinitrodil
CAS Number:143248-63-9
Molecular formula:C10H10N2O5
Molecular Weight:238.198

24207-38-3
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143248-63-9
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) p-toluenesulfonic acid, 2.) 3N aq. HCl / 1.) toluene, 2 h, reflux, 2.) THF, 24 h, reflux
2: 95 percent / thionyl chloride / CHCl₃ / 3 h / Heating
3: 88 percent / silver nitrate / acetonitrile / 2 h / Heating

References:

Benedini, Francesca;Bertolini, Giorgio;Cereda, Roberta;Dona, Giancarlo;Gromo, Gianni;et al. [Journal of Medicinal Chemistry,1995,vol. 38,# 1,p. 130 - 136]

4H-1,3-Benzoxazin-4-one, 3-(2-chloroethyl)-2,3-dihydro-

143248-55-9
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143248-63-9
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References

119-36-8 Synthesis

119-36-8
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143248-63-9
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References

4H-1,3-Benzoxazin-4-one, 2,3-dihydro-3-(2-hydroxyethyl)-

143248-47-9
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143248-63-9
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References

4H-1,3-Benzoxazin-4-one, 3-[2-(acetyloxy)ethyl]-2,3-dihydro-

143248-39-9
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143248-63-9
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References

Sinitrodil Related Search:

Diltiazem Fasudil hydrochloride Aminoethyl nitrate

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