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879001-62-4

tert-butyl 2-fluoro-2-methylpropylcarbamate synthesis

3synthesis methods
-

Yield:879001-62-4 86%

Reaction Conditions:

with 2,6-dimethylpyridine;4,4'-dimethoxy-2,2'-bipyridine;ferrous acetate;1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in lithium hydroxide monohydrate;acetonitrile at 20; for 2 h;Schlenk technique;Inert atmosphere;Sealed tube;Irradiation;

References:

Zhang, Yu;Qian, Jiahui;Wang, Miao;Huang, Yahao;Hu, Peng [Organic Letters,2022,vol. 24,# 32,p. 5972 - 5976] Location in patent:supporting information