tert-butyl 4-(phenylthio)piperidine-1-carboxylate synthesis
- Product Name:tert-butyl 4-(phenylthio)piperidine-1-carboxylate
- CAS Number:154612-64-3
- Molecular formula:C16H23NO2S
- Molecular Weight:293.42
Yield:154612-64-3 87%
Reaction Conditions:
Stage #1: thiophenolwith sodium hydride in N,N-dimethyl-formamide at 25; for 0.5 h;
Stage #2: tert-butyl 4-bromo-1-piperidinecarboxylate in N,N-dimethyl-formamide at 80; for 1 h;
References:
Brauns, Marcus;Cramer, Nicolai [Angewandte Chemie - International Edition,2019,vol. 58,# 26,p. 8902 - 8906][Angew. Chem.,2019,vol. 131,p. 8994 - 8998,5] Location in patent:supporting information
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