tert-Butyl(imino)methyl-lambda6-sulfanone synthesis
- Product Name:tert-Butyl(imino)methyl-lambda6-sulfanone
- CAS Number:1085526-21-1
- Molecular formula:C5H13NOS
- Molecular Weight:135.23
6163-64-0
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Yield:1085526-21-1 0.416 g
Reaction Conditions:
with ammonium carbamate;[bis(acetoxy)iodo]benzene in methanol at 20;
Steps:
Intermediate 16: Synthesis of Compound P1
Compound P1-1 (0.5 g), methanol (10 mL), ammonium carbamate (0.56 g) and iodobenzene diacetate (3.09 g) were mixed and reacted at room temperature for 5 hours. The reaction solution was filtered and concentrated, and the obtained crude product was separated and purified by column chromatography (dichloromethane:methanol=16:1) to obtain compound P1 (0.416g).
References:
WO2022/237875,2022,A1 Location in patent:Page/Page column 26-27
75-97-8
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14094-11-2
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