ChemicalBook CAS DataBase List tetrahydrofuro[2,3-b]furan-2(3H)-one

tetrahydrofuro[2,3-b]furan-2(3H)-one synthesis

2synthesis methods

Product Name:tetrahydrofuro[2,3-b]furan-2(3H)-one
CAS Number:104223-37-2
Molecular formula:C6H8O3
Molecular Weight:128.1259

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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 88 percent / pyridine / CHCl₃ / 2 h
2.1: 81 percent / dimethylformamide / 18 h / 70 °C
3.1: aq. NaOH / 2.5 h / Heating
3.2: 91 percent / aq. HCl / 1.5 h / 20 °C / pH 1

References:

Meulemans, Tommi M.;Stork, Gerrit A.;Macaev, Fliur Z.;Jansen, Ben J. M.;De Groot, Aede [Journal of Organic Chemistry,1999,vol. 64,# 25,p. 9178 - 9188]

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References

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