TETRAKIS(TRICHLOROSILYL)SILANE synthesis
- Product Name:TETRAKIS(TRICHLOROSILYL)SILANE
- CAS Number:50350-62-4
- Molecular formula:Cl12Si5
- Molecular Weight:565.86
13465-77-5
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50350-62-4
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Yield:50350-62-4 80%
Reaction Conditions:
in neat (no solvent);byproducts: SiCl3(SiCl3)(Me2NC2H4NMe2); Si2Cl6 was heated in presence of SiCl3(SiCl3)(Me2NC2H4NMe2) (catalyst) at 55°C for 15 h; NMR monitoring; filtered; evapd. (vac.);
References:
Tillmann, Jan;Meyer-Wegner, Frank;Nadj, Andor;Becker-Baldus, Johanna;Sinke, Tanja;Bolte, Michael;Holthausen, Max C.;Wagner, Matthias;Lerner, Hans-Wolfram [Inorganic Chemistry,2012,vol. 51,# 15,p. 8599 - 8606]
13596-23-1
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50350-62-4
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