ChemicalBook CAS DataBase List TG6-10-1

TG6-10-1 synthesis

2synthesis methods

Product Name:TG6-10-1
CAS Number:1415716-58-3
Molecular formula:C23H23F3N2O4
Molecular Weight:448.43

51310-54-4
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1415716-58-3
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C
1.2: 0 - 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 8 h / 20 °C

References:

Ganesh, Thota;Jiang, Jianxiong;Yang, Myung-Soon;Dingledine, Ray [Journal of Medicinal Chemistry,2014,vol. 57,# 10,p. 4173 - 4184]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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1415716-58-3
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$29.00/1mg

References