Thiazolo[5,4-d]thiazole-2,5-dicarboxylicacid synthesis

3synthesis methods

Product Name:Thiazolo[5,4-d]thiazole-2,5-dicarboxylicacid
CAS Number:27492-59-7
Molecular formula:C6H2N2O4S2
Molecular Weight:230.22

2,5-di(furan-2-yl)[1,3]thiazolo[5,4-d][1,3]thiazole

27396-05-0
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Thiazolo[5,4-d]thiazole-2,5-dicarboxylicacid

27492-59-7
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Yield:27492-59-7 85%

Reaction Conditions:

Stage #1: 2,5-bis(2-furyl)thiazolo<5,4-d>thiazolewith potassium permanganate;Aliquat 336 in tert-butyl alcohol at 20; for 18 h;
Stage #2: with hydrogenchloride pH=0 - 1; for 0.5 h;Further stages.;

References:

Benin, Vladimir;Yeates, Alan T.;Dudis, Douglas [Journal of Heterocyclic Chemistry,2008,vol. 45,# 3,p. 811 - 819]

Thiazolo[5,4-d]thiazole, 2,5-bis(2-phenylethenyl)-

27396-04-9
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27492-59-7
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References

Thiazolo[5,4-d]thiazole-2,5-dicarboxylic acid, 2,5-diethyl ester

27484-49-7
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27492-59-7
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References

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