tributyl(1-fluorovinyl)stannane synthesis
- Product Name:tributyl(1-fluorovinyl)stannane
- CAS Number:157437-37-1
- Molecular formula:C14H29FSn
- Molecular Weight:335.09
56-35-9
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Yield:157437-37-1 76%
Reaction Conditions:
cesium fluoride in N,N-dimethyl-formamide;Sonication; Sn oxide (0.6 equiv.) and CsF (0.1 equiv.) were added to soln. of Si compd. in DMF at room temp. under Ar; mixt. was ultrasonic irradiated for 10 min; mixt. quenched with water; extd. (hexane/ether, 3/1); dried (Na2SO4); concd.; residue chromd. (silica gel, hexane); elem. anal.;
References:
Hanamoto, Takeshi;Handa, Kumiko;Mido, Tomonori [Bulletin of the Chemical Society of Japan,2002,vol. 75,# 11,p. 2497 - 2502]