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ChemicalBook CAS DataBase List TRIPHENYLLEAD CHLORIDE

TRIPHENYLLEAD CHLORIDE synthesis

4synthesis methods
Vanadium, hexacarbonyl(triphenylplumbyl)-, (OCF-7-1-222222)-

89669-25-0
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21050-13-5 Synthesis
Bis(triphenylphosphine)iminium chloride

21050-13-5
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$15.00/5g

Phosphorus(1+), triphenyl(P,P,P-triphenylphosphine imidato-N)-, (T-4)-, (OC-6-11)-hexacarbonylvanadate(1-) (9CI)

38856-17-6
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Yield:38856-17-6 97% ,1153-06-6 86%

Reaction Conditions:

in dichloromethane;under N2 or Ar, exclusion of light; evapn. of solvent, extn. (hot toluene), sepn. of PPN(V(CO)6), evapn. of soln. (Ph3PbCl);

References:

Calderazzo, Fausto;Pampaloni, Guido;Pelizzi, Giancarlo;Vitali, Francesca [Polyhedron,1988,vol. 7,p. 2039 - 2048]

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