Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
logo
Inquriy
Try our best to find the right business for you.
Messages
Do not miss inquiry messages Please log in to view all inquiry messages.
My chemicalbook

Welcome back!

Structured search
18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List TRIPTYCENE
477-75-8

TRIPTYCENE synthesis

7synthesis methods
Triptycene can be prepared in one step in 28% yield from the Diels–Alder reaction of anthracene and benzyne. In this method, benzyne is generated by the reaction of magnesium and 2-bromofluorobenzene.
Benzene, 1-methyl-2,3-bis(trimethylsilyl)-

101300-65-6
0 suppliers
inquiry

TRIPTYCENE

477-75-8
146 suppliers
$9.00/250mg

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 86 percent / CH2Cl2 / 2 h / 20 °C
2: 100 percent / Bu4NF / CH2Cl2; tetrahydrofuran / 0.5 h / 20 °C

References:

Kitamura, Tsugio;Yamane, Masakatsu;Inoue, Kensuke;Todaka, Mitsuru;Fukatsu, Norihiko;Meng, Zhaohong;Fujiwara, Yuzo [Journal of the American Chemical Society,1999,vol. 121,# 50,p. 11674 - 11679]

120-12-7 Synthesis
Anthracene

120-12-7
341 suppliers
$10.00/5g

Anthranilic acid

118-92-3
0 suppliers
$23.00/250g

TRIPTYCENE

477-75-8
146 suppliers
$9.00/250mg

References
9,10-Dihydro-9,10-[1,2]benzenoanthracene-9-yl bromide

15364-55-3
31 suppliers
$125.00/1g

TRIPTYCENE

477-75-8
146 suppliers
$9.00/250mg

Lithium, 9,10[1',2']-benzenoanthracen-9(10H)-yl- (9CI)

59239-90-6
0 suppliers
inquiry

References
9,10-Dihydro-9,10-[1,2]benzenoanthracene-9-yl bromide

15364-55-3
31 suppliers
$125.00/1g

TRIPTYCENE

477-75-8
146 suppliers
$9.00/250mg

References
9,10[1',2']-Benzenoanthracene-1,4-diamine, 9,10-dihydro-

88849-55-2
0 suppliers
inquiry

TRIPTYCENE

477-75-8
146 suppliers
$9.00/250mg

References