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ChemicalBook CAS DataBase List Tris(3,5-dimethyl-1-pyrazolyl)methane
28791-97-1

Tris(3,5-dimethyl-1-pyrazolyl)methane synthesis

1synthesis methods
-

Yield:28791-97-1 65%

Reaction Conditions:

Stage #1: 3,5-dimethyl-1H-pyrazolewith tetrabutylammomium bromide;sodium carbonate in water;deprotonation;
Stage #2: chloroform in water; for 3 h;Heating;Substitution;

References:

Reger, Daniel L.;Grattan, T. Christian;Brown, Kenneth J.;Little, Christine A.;Lamba, Jaydeep J.S.;Rheingold, Arnold L.;Sommer, Roger D. [Journal of Organometallic Chemistry,2000,vol. 607,# 1-2,p. 120 - 128]