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ChemicalBook CAS DataBase List VINYLTRIETHYLGERMANE
6207-41-6

VINYLTRIETHYLGERMANE synthesis

2synthesis methods
-

Yield:6207-41-6 82%

Reaction Conditions:

in tetrahydrofuran;(Ar); soln. of Mg compd. in THF was added dropwise to soln. of Ge compd.in THF; stirred at 45°C for 24 h; washed (H2O, Et2O); dried (CaCl2); distd.;

References:

Marciniec, Bogdan;LAwicka, Hanna;Dudziec, Beata [Organometallics,2007,vol. 26,# 21,p. 5188 - 5192]