ChemicalBook CAS DataBase List (Z)-3,3-DIMETHYLCYCLOHEXYLIDENEETHANOL

(Z)-3,3-DIMETHYLCYCLOHEXYLIDENEETHANOL synthesis

8synthesis methods

Product Name:(Z)-3,3-DIMETHYLCYCLOHEXYLIDENEETHANOL
CAS Number:26532-23-0
Molecular formula:C10H18O
Molecular Weight:154.25

(E)-2-(3,3-Dimethylcyclohexylidene)-ethanol

30346-27-1
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26532-23-0
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 93 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 15 h / Ambient temperature
2: 80percent m-ClC₆H₄COOOH / CH₂Cl₂ / 2 h / Ambient temperature
3: 1.) 0.75M lithium diphenylphosphide, 2.) MeI / 1.) THF, 1 h, 25 deg C, 2.) 1 h, RT
4: 82 percent / pyridinium p-toluenesulfonate / ethanol / 3 h / 55 °C

References:

Mori, Kenji;Itou, Masamichi [Liebigs Annalen der Chemie,1989,p. 969 - 974]

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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26532-23-0
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References

(Z)-(3,3-Dimethylcyclohexylidene)acetic acid methyl ester

30346-23-7
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26532-23-0
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References

1000210-73-0
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26532-23-0
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References

1000210-73-0
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26532-23-0
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References