Z-9-TETRADECENAL synthesis
- Product Name:Z-9-TETRADECENAL
- CAS Number:53939-27-8
- Molecular formula:C14H26O
- Molecular Weight:210.36
3927-60-4
47 suppliers
inquiry
53939-27-8
28 suppliers
inquiry
Yield:-
Steps:
Multi-step reaction with 9 steps
1: 36.3 percent / Pb(OAc)4, pyridine, Cu(OAc)2 / benzene / 3 h / Heating
2: 1) Br2, 2) aq.KOH / 1) CCl4, r.t., 2) 135-145 deg C, 4 h
3: 100 percent / conc.H2SO4 / 4 h / Heating
4: 83 percent / LAH / diethyl ether / 2 h / Ambient temperature
5: 98 percent / PPTS / CH2Cl2 / 4 h / Ambient temperature
6: 1) n-BuLi, 2) HMPT / 1) THF, hexane, 10 deg C, 2) <25 deg C, 0.5 h
7: 92 percent / PPTS / ethanol / 70 °C
8: 98 percent / H2, quinoline / 5percent Pd/BaSO4 / methanol
9: 89 percent / PCC / CH2Cl2 / 1.5 h
References:
Ranganathan, S.;Maniktala, Vibha;Kumar, Raaj;Singh, G. P. [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1984,vol. 23,# 12,p. 1197 - 1207]
35153-15-2
68 suppliers
inquiry
53939-27-8
28 suppliers
inquiry
3930-10-7
0 suppliers
inquiry
53939-27-8
28 suppliers
inquiry
19754-58-6
2 suppliers
inquiry
53939-27-8
28 suppliers
inquiry
1642-49-5
33 suppliers
inquiry
53939-27-8
28 suppliers
inquiry