(Z)-benzyl but-2-enoate(WXC06956) synthesis
1synthesis methods
- Product Name:(Z)-benzyl but-2-enoate(WXC06956)
- CAS Number:92758-75-3
- Molecular formula:C11H12O2
- Molecular Weight:176.21
Yield:92758-75-3 96%
Reaction Conditions:
Stage #1: (Z)-but-2-enoic acidwith potassium carbonate in N,N-dimethyl-formamide at 22; for 0.333333 h;Inert atmosphere;
Stage #2: benzyl bromide in N,N-dimethyl-formamide at 22; for 12 h;Inert atmosphere;
References:
Liu, Zhenxing;Xu, Chaofan;Del Pozo, Juan;Torker, Sebastian;Hoveyda, Amir H. [Journal of the American Chemical Society,2019,vol. 141,# 17,p. 7137 - 7146] Location in patent:supporting information