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ChemicalBook CAS DataBase List zirconocene
12116-83-5

zirconocene synthesis

2synthesis methods
1291-32-3 Synthesis
Bis(cyclopentadienyl)zirconium dichloride

1291-32-3
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$10.00/1g

zirconocene

12116-83-5
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Yield:12116-83-5 88%

Reaction Conditions:

with sodium in tetrahydrofuran;reduction (Na in naphthalene); protective gas: O2-free He;; sublimation (150°C/1E-3 Torr/several hours);;

References:

Wailes, P. C.;Weigold, H. [Journal of Organometallic Chemistry,1970,vol. 24,p. 713 - 715] Watt, G. W.;Drummond, F. O. [Journal of the American Chemical Society,1966,vol. 88,p. 5926 - 5927]