ChemicalBook--->CAS DataBase List--->52986-70-6

52986-70-6

52986-70-6 Structure

52986-70-6 Structure
IdentificationMore
[Name]

6-Methoxyisoquinoline
[CAS]

52986-70-6
[Synonyms]

6-METHOXY-ISOQUINOLINE
6-Methoxyisoquinoline 90%
[Molecular Formula]

C10H9NO
[MDL Number]

MFCD04114861
[Molecular Weight]

159.18
[MOL File]

52986-70-6.mol
Chemical PropertiesBack Directory
[Appearance]

Clear Oil
[Boiling point ]

88-95?C/0.8 Torr
[density ]

1.130±0.06 g/cm3(Predicted)
[storage temp. ]

Sealed in dry,Room Temperature
[solubility ]

Chloroform, Dichloromethane
[form ]

Oil
[pka]

6.11±0.10(Predicted)
[color ]

Pale Yellow
[CAS DataBase Reference]

52986-70-6(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Hazard Note ]

Irritant
[HS Code ]

2933499090
Hazard InformationBack Directory
[Chemical Properties]

Clear Oil
[Uses]

6-Methoxy Isoquinoline (cas# 52986-70-6) is a compound useful in organic synthesis.
[Preparation]

6-Methoxyisoquinoline synthesis: Using benzaldehyde as the starting material, m-methoxybenzaldehyde is obtained through nitration, reduction, diazotization, hydrolysis and methylation, and 3-methoxybenzaldehyde is obtained through condensation with nitromethane Shiff base and reduction of aluminum hydride -p-Phenylethylamine. The Pictet-Spengler reaction of 3-methoxyl-p-phenylethylamine and 40% aqueous formaldehyde produces 6-methoxyl-1,2,3,4-tetrahydroisoquinoline, and then obtains the target compound in dehydrogenation 6-Methoxyisoquinoline.
[Synthesis Reference(s)]

Journal of the American Chemical Society, 69, p. 1939, 1947 DOI: 10.1021/ja01200a028
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