11β,16α,17,21-Tetrahydroxypregna-1,4-dien-3,20-dion

11β,16α,17,21-Tetrahydroxypregna-1,4-dien-3,20-dion Chemische Eigenschaften,Einsatz,Produktion Methoden

Chemische Eigenschaften

White Crystalline Solid

Synthese

501 g of crude 16α-hydroxy prednisolone acetate is dissolved in 700 ml of dichloromethane and 700 ml of ethanol, then 1.5 ml of formic acid is added, 24 ml of 5% sodium hypochlorite aqueous solution is added dropwise, and the temperature is controlled at 15 °C, and the reaction is stirred to obtain the preliminary processed product; Add 150 ml of 5% sodium bisulfite aqueous solution to the above-mentioned preliminary treatment product, concentrate on removing the solvent, adding water to hydrolyze, and filter to obtain 45 g of 16α-hydroxyprednisolone acetate refined product; 45 g of 16α-hydroxyprednisolone acetate obtained above was dissolved in a mixed organic solvent of 250 ml of dichloromethane and 250 ml of methanol, stirred and cooled to 0 °C, 90 ml of 10% sodium sulfite aqueous solution was added, and the reaction was stirred. After completion, it was neutralized with 15% sulfuric acid by mass concentration; the mixed organic solvent was concentrated, watered out, filtered, and dried to obtain 36.5 g of 16α-hydroxyprednisolone (11β,16α,17,21-tetrahydroxypregna-1,4-diene-3,20-dione).

11β,16α,17,21-Tetrahydroxypregna-1,4-dien-3,20-dion Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

11β,16α,17,21-Tetrahydroxypregna-1,4-dien-3,20-dion Anbieter Lieferant Produzent Hersteller Vertrieb Händler.

Firmenname	Telefon	E-Mail	Land	Produktkatalog	Edge Rate
BIONNA MEDICINE CO.,LTD	01056380788-8515; +8618518759099	790226113@qq.com	China	52	58
Zibo Hangyu Biotechnology Development Co., Ltd	+86-0533-2185556 +8617865335152	Mandy@hangyubiotech.com	China	11013	58
Capot Chemical Co.,Ltd.	571-85586718 +8613336195806	sales@capotchem.com	China	29797	60
Shanghai Daken Advanced Materials Co.,Ltd	+86-371-66670886	info@dakenam.com	China	15932	58
Beijing Cooperate Pharmaceutical Co.,Ltd	010-60279497	sales01@cooperate-pharm.com	CHINA	1811	55
Henan Tianfu Chemical Co.,Ltd.	+86-0371-55170693 +86-19937530512	info@tianfuchem.com	China	21691	55
Hangzhou FandaChem Co.,Ltd.	008657128800458; +8615858145714	fandachem@gmail.com	China	9346	55
Hubei XinRunde Chemical Co., Ltd.	+8615102730682	bruce@xrdchem.cn	CHINA	566	55
career henan chemical co	+86-0371-86658258	sales@coreychem.com	China	29914	58
Accela ChemBio Inc.	(+1)-858-699-3322	info@accelachem.com	United States	19965	58

13951-70-7(11β,16α,17,21-Tetrahydroxypregna-1,4-dien-3,20-dion)Verwandte Suche:

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• 16A-HYDROXY-PREDNISONLONE
• 11beta,16alpha,17,21-tetrahydroxypregna-1,4-diene-3,20-dione
• 16 Alpha Hydroxprednisolone
• 16α-HYDROXY-PREDNISONLONE
• 11,16a,17a,21-Tetrahydroxypregna-1,4-diene-3,20-dione
• Einecs 237-731-1
• 16A-HYDROXY-PREDNISOLONE
• 11a,16b,17,21-tetrahydroxy-pregna-1,4-diene-3,20-dione
• 11B,16A,17A,21-TETRAHYDROXYPREGNA-1,4-DIENE-3,20-DIONE
• 16a-Hydroxypredisolone
• (11β,16α)-11,16,17,21-Tetrahydroxypregna-1,4-diene-3,20-dione
• 16α-Hydroxyprednisolon
• Budesonide IMpurity A (16-alpha-Hydroxy-Prednisolone)
• (8S,9S,10R,13S,14S,16R,17S)-11,16,17-Trihydroxy-17-(2-hydroxyacetyl)-10,13-dimethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-3-one
• Prednisolone impurity 1/Prednisolone EP Impurity A/16-alpha-Hydroxy-Prednisolone/11?,16a,17,21-Tetrahydroxypregna-1,4-diene-3,20-dione
• 9-[3-(1,2-dihydroxyheptyl)-2-oxiranyl]-9-hydroxynonanoic acid
• Budesonide iMpurit A
• Budesonide EP Impurity A (16-alpha-Hydroxy-Prednisolone)
• BNKY015-BD04
• Budesonide EP Impurity A
• 16b
• 20-dione
• 21-Tetrahydroxy-pregna-1
• 4-diene-3
• Budesonide impurity A
• Budesonide Impurity 1(Budesonide EP Impurity A)
• 11beta,16alpha,17,21-Tetrahydroxypr
• Pregna-1,4-diene-3,20-dione, 11,16,17,21-tetrahydroxy-, (11β,16α)-
• Desonide Impurity A
• 16α-hydroxy Prednisolone
• 11a,16b,17,21-Tetrahydroxy-pregna-1,4-diene-3,20-dione USP/EP/BP
• Tmo Trimethylamine N-Oxide Dihydrate Powder
• 16α-hydroxy-prednisonlone
• 16 α Hydroxy PrednisoloneQ: What is 16 α Hydroxy Prednisolone Q: What is the CAS Number of 16 α Hydroxy Prednisolone Q: What is the storage condition of 16 α Hydroxy Prednisolone
• 16α-Hydroxyprednisolone-d5
• 11β,16α,17α,21-tetrahydroxy-1,4-pregnadiene-3,20-dione(triamcinolone)
• 11β,16α,17,21-Tetrahydroxypregna-1,4-diene-3,20-dione
• 11β,16α,17α,21-Tetrahydroxypregna-1,4-diene-3,20-dione
• 16-ALPHA-HYDROXY PREDNISOLONE
• 11β,16α,17,21-tetrahydroxypregna-1,4-diene-3,20-dione
• 16α-hydroxy-prednisolone
• (8S,9S,10R,11S,13S,14S,16R,17S)-11,16,17-trihydroxy-17-(2-hydroxyacetyl)-10,13-diMethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthren-3-one
• 16α-Hydroeyprednisolone
• Pregna-1,4-diene-3,20-dione, 11,16,17,21-tetrahydroxy-, (11β,16α)-
• 16α-Hydroxyprednisolone (Budesonide Impurity)
• 11β,16α,17α,21-Tetrahydroxypregnα-1,4-diene-3,20-dione
• Desonide EP Impurity-A
• 11-Beta,16-Alpha,17-Alpha,21-Tetrahydroxypregna-1,4-diene-3,20-dione
• 11β,16α,17α,21-tetrahydroxyprogesterone-1,4-diene-3,20-dione
• (8S,9S,10R,11S,13S,14S,16R,17S)-11,16,17-trihydroxy-17-(2-hydroxyacetyl)-10,13-dimethyl-7,8,9,11,12,14,15,16-octahydro-6H-cyclopenta[a]phenanthren-3-one
• 13951-70-7
• 13952-70-7
• Pharmaceutical Raw Materials
• Metabolites & Impurities
• Intermediates & Fine Chemicals
• Metabolites
• Pharmaceuticals
• Steroids