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3-Bromophthalide

CAS No.
6940-49-4
Chemical Name:
3-Bromophthalide
Synonyms
TALM-002;3-BromophthaL;BROMOPHTHALIDE;3-Bromophtalide;3-BROMOPHTHALIDE;3-bromophthalein;3-Bromophthalide97%;3-Bromophthalide 3-;3-Bromophthalide >3-BROMOPHTHALIDE 98+%
CBNumber:
CB3157574
Molecular Formula:
C8H5BrO2
Molecular Weight:
213.03
MDL Number:
MFCD00040520
MOL File:
6940-49-4.mol
MSDS File:
SDS
Last updated:2024-09-02 15:48:56

3-Bromophthalide Properties

Melting point 86°C
Boiling point 138 °C / 3mmHg
Density 1.768±0.06 g/cm3(Predicted)
storage temp. under inert gas (nitrogen or Argon) at 2–8 °C
solubility soluble in Methanol
form powder to crystal
color White to Light yellow to Light orange
InChIKey CLMSHAWYULIVFQ-UHFFFAOYSA-N
CAS DataBase Reference 6940-49-4(CAS DataBase Reference)
EPA Substance Registry System 1(3H)-Isobenzofuranone, 3-bromo- (6940-49-4)

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319
Precautionary statements  P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313
Risk Statements  38-41
Safety Statements  26-36/37/39
HS Code  2932209090
NFPA 704
1
1 0

3-Bromophthalide price More Price(19)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical B1068 3-Bromophthalide >98.0%(T) 6940-49-4 5g $55 2024-03-01 Buy
TCI Chemical B1068 3-Bromophthalide >98.0%(T) 6940-49-4 25g $144 2024-03-01 Buy
Oakwood 113900 3-Bromophthalide 97% 6940-49-4 100g $390 2021-12-16 Buy
Biosynth Carbosynth FB33933 3-Bromophthalide 6940-49-4 250g $292.5 2021-12-16 Buy
Biosynth Carbosynth FB33933 3-Bromophthalide 6940-49-4 50g $67.5 2021-12-16 Buy
Product number Packaging Price Buy
B1068 5g $55 Buy
B1068 25g $144 Buy
113900 100g $390 Buy
FB33933 250g $292.5 Buy
FB33933 50g $67.5 Buy

3-Bromophthalide Chemical Properties,Uses,Production

Synthesis

3-Bromophthalide is produced by reacting phthalide with N-bromosuccinimide in carbon tetrachloride solution.
Ten grams (0.075 mole) of phthalide (Note 1), 13.3 g. (0.075 mole) of N-bromosuccinimide, and 200 ml. of dry carbon tetrachloride are refluxed for 30 minutes in a 500-ml. flask carrying a reflux condenser equipped with a drying tube containing Drierite. The reaction mixture is exposed to the light of an ordinary 100-watt unfrosted light bulb placed 6–8 in. from the flask. The end of the reaction is indicated by the disappearance of N-bromosuccinimide from the bottom of the flask and accumulation of succinimide at the top of the reaction mixture. The succinimide is removed by filtration and the filtrate concentrated under atmospheric pressure to 15–20 ml. Cooling of this concentrate followed by filtration gives 12–13 g. (75–81%) of crude 3-bromophthalide, m.p. 74–80°. The crude material, when recrystallized from cyclohexane, gives colorless plates, m.p. 78–80°.
3-Bromophthalide synthesis

3-Bromophthalide Preparation Products And Raw materials

Raw materials

Preparation Products

Global( 255)Suppliers
Supplier Tel Email Country ProdList Advantage
Capot Chemical Co.,Ltd.
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View Lastest Price from 3-Bromophthalide manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
Butyphthalide impurity 88 pictures 2024-09-20 Butyphthalide impurity 88
6940-49-4
US $0.00-0.00 / mg 10mg 0.98 5g ShenZhen H&D Pharmaceutical Technology Co., LTD
3-Bromophthalide pictures 2021-10-09 3-Bromophthalide
6940-49-4
US $10.00 / KG 1KG 99% 20 tons Hebei Zhanyao Biotechnology Co. Ltd
3-Bromophthalide pictures 2021-07-13 3-Bromophthalide
6940-49-4
US $15.00-10.00 / KG 1KG 99%+ HPLC Monthly supply of 1 ton Zhuozhou Wenxi import and Export Co., Ltd
  • 3-Bromophthalide pictures
  • 3-Bromophthalide
    6940-49-4
  • US $15.00-10.00 / KG
  • 99%+ HPLC
  • Zhuozhou Wenxi import and Export Co., Ltd
3-BROMO-1(3H)-ISOBENZOFURANONE 3-BROMOPHTHALIDE 3-bromo-1(3h)-isobenzofuranon 3-Bromophtalide 3-Bromophthalide97% 1(3H)-Isobenzofuranone, 3-bromo- BROMOPHTHALIDE 3-BROMOPHTHALIDE 98+% 3-Bromoisobenzofuran-1(3H)-one 3-BROMOPHTHALIDE, 96%+ 3-BROMOPHTHALIDE Talampicillin TALM-002 3-Bromophthalide 3- 3-BromophthaL 3-Bromophthalide > 3-bromophthalein Butyphthalide impurity 88 6940-49-4 6490-49-4 940-49-4 Phthalides bc0001