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Tris(4-methoxyphenyl)phosphine

Tris(4-methoxyphenyl)phosphine Structure
Tris(4-methoxyphenyl)phosphine structure
CAS No.
855-38-9
Chemical Name:
Tris(4-methoxyphenyl)phosphine
Synonyms
tris(4-Methoxyphenyl)phosphane;TRIS(P-METHOXYPHENYL)PHOSPHINE;Trianisylphosphine;TRIS(P-METHOXYP;Tris(4-methoxyphenyL;Tri-p-anisylphosphine;LABOTEST-BB LTBB005439;TRIS(P-ANISYL)PHOSPHINE;Tri(p-methoxyphenyl)phosphine;TRI(4-METHOXYPHENYL)PHOSPHINE
CBNumber:
CB8228460
Molecular Formula:
C21H21O3P
Molecular Weight:
352.36
MDL Number:
MFCD00014896
MOL File:
855-38-9.mol
Last updated:2024-03-08 15:18:56
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Tris(4-methoxyphenyl)phosphine Properties

Melting point 131-134 °C (lit.)
Boiling point 457.8±40.0 °C(Predicted)
Density 1.1352 (estimate)
storage temp. Inert atmosphere,Room Temperature
form Crystalline Powder
color White to pale yellow
Water Solubility Insoluble in water.
Sensitive Air Sensitive
BRN 2815911
InChI InChI=1S/C21H21O3P/c1-22-16-4-10-19(11-5-16)25(20-12-6-17(23-2)7-13-20)21-14-8-18(24-3)9-15-21/h4-15H,1-3H3
InChIKey UYUUAUOYLFIRJG-UHFFFAOYSA-N
SMILES P(C1=CC=C(OC)C=C1)(C1=CC=C(OC)C=C1)C1=CC=C(OC)C=C1
CAS DataBase Reference 855-38-9(CAS DataBase Reference)
FDA UNII PF5BT47LZ8
EPA Substance Registry System Phosphine, tris(4-methoxyphenyl)- (855-38-9)

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P264-P271-P280-P302+P352-P305+P351+P338
Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-37/39-24/25
WGK Germany  3
TSCA  Yes
HS Code  29319090
NFPA 704
0
2 0

Tris(4-methoxyphenyl)phosphine price More Price(33)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 395102 Tris(4-methoxyphenyl)phosphine 95% 855-38-9 1g $62.6 2024-03-01 Buy
Sigma-Aldrich 395102 Tris(4-methoxyphenyl)phosphine 95% 855-38-9 5g $164 2024-03-01 Buy
TCI Chemical T0861 Tris(4-methoxyphenyl)phosphine >97.0%(T) 855-38-9 5g $107 2024-03-01 Buy
TCI Chemical T0861 Tris(4-methoxyphenyl)phosphine >97.0%(T) 855-38-9 25g $324 2024-03-01 Buy
Alfa Aesar A15596 Tris(4-methoxyphenyl)phosphine 98% 855-38-9 1g $41.1 2024-03-01 Buy
Product number Packaging Price Buy
395102 1g $62.6 Buy
395102 5g $164 Buy
T0861 5g $107 Buy
T0861 25g $324 Buy
A15596 1g $41.1 Buy

Tris(4-methoxyphenyl)phosphine Chemical Properties,Uses,Production

Chemical Properties

White to pale yellow crystalline powder

Uses

suzuki reaction

Uses

Tris(4-methoxyphenyl)phosphine is a useful intermediate employed in organic synthesis and in other chemical processes.

Application

Tris(4-methoxyphenyl)phosphine is used as a ligand in organometallic chemistry and homogeneous catalysis.
This compound is suitable for the following reaction types: Buchwald-Hartwig Cross Coupling Reaction, Heck Reaction, Hiyama Coupling, Negishi Coupling, Sonogashira Coupling, Stille Coupling, Suzuki-Miyaura Coupling, and Cross Couplings.

Synthesis

To a solution of tertiary phosphine oxides 2 (0.4mmol) in CH2Cl2 (2mL) was added oxalyl chloride (0.4mmol) dropwise at room temperature under an argon atmosphere. After 30 minutes, HEH (1mmol) was added to the mixture in one portion, and TEA (3mmol) was added. The mixture was stirred for another 2h at 40°C and then diluted with H2O (10mL). The resulting mixture was extracted with CH2Cl2 repeatedly. The extracts were dried (anhydrous Na2SO4) and evaporated. The crude product was purified by column chromatography on silica gel using ethyl acetate/petroleum ether to afford the pure product Tris(4-methoxyphenyl)phosphine.

Tris(4-methoxyphenyl)phosphine Preparation Products And Raw materials

Raw materials

Preparation Products

Tris(4-methoxyphenyl)phosphine Suppliers

Global( 236)Suppliers
Supplier Tel Email Country ProdList Advantage
Shaoxin Catsyn Co., Ltd.
+undefined-0575-82040869 +86-0575-82040869; sales@catsyn.com China 6116 58
Capot Chemical Co.,Ltd. 		571-85586718 +8613336195806 sales@capotchem.com China 29797 60
Shanghai Daken Advanced Materials Co.,Ltd 		+86-371-66670886 info@dakenam.com China 15928 58
Henan Tianfu Chemical Co.,Ltd. 		+86-0371-55170693 +86-19937530512 info@tianfuchem.com China 21691 55
career henan chemical co 		+86-0371-86658258 sales@coreychem.com China 29914 58
Jinan Carbotang Biotech Co.,Ltd. 		+8615866703830 figo.gao@foxmail.com China 6992 58
Hubei Jusheng Technology Co.,Ltd. 		18871490254 linda@hubeijusheng.com CHINA 28180 58
Accela ChemBio Inc. 		(+1)-858-699-3322 info@accelachem.com United States 19965 58
Wuhan Pengo Technology.,Ltd. 		+86-27-81330736 +86-13628634921 sunny.w@boronicgroup.com CHINA 171 58
Chongqing Chemdad Co., Ltd 		+86-023-61398051 +8613650506873 sales@chemdad.com China 39916 58
Supplier Advantage
Shaoxin Catsyn Co., Ltd.
58
Capot Chemical Co.,Ltd. 		60
Shanghai Daken Advanced Materials Co.,Ltd 		58
Henan Tianfu Chemical Co.,Ltd. 		55
career henan chemical co 		58
Jinan Carbotang Biotech Co.,Ltd. 		58
Hubei Jusheng Technology Co.,Ltd. 		58
Accela ChemBio Inc. 		58
Wuhan Pengo Technology.,Ltd. 		58
Chongqing Chemdad Co., Ltd 		58

View Lastest Price from Tris(4-methoxyphenyl)phosphine manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
Tris(4-Methoxyphenyl)phosphine pictures 2023-01-31 Tris(4-Methoxyphenyl)phosphine
855-38-9
 US $0.00 / G 500G 98%min 30kg/month WUHAN FORTUNA CHEMICAL CO., LTD
Tris(p-Methoxyphenyl)phosphine pictures 2020-03-16 Tris(p-Methoxyphenyl)phosphine
855-38-9
 US $1.00-0.00 / KG 1KG 99% 20 tons Shaanxi Dideu Medichem Co. Ltd
TRIS(4-METHOXYPHENYL)PHOSPHINE pictures 2019-07-06 TRIS(4-METHOXYPHENYL)PHOSPHINE
855-38-9
 US $1.00 / KG 1KG 99% 1MT Career Henan Chemical Co

Tris(4-methoxyphenyl)phosphine Spectrum

TRIS(4-METHOXYPHENYL)PHOSPHINE(855-38-9)MSTRIS(4-METHOXYPHENYL)PHOSPHINE(855-38-9)1HNMRTRIS(4-METHOXYPHENYL)PHOSPHINE(855-38-9)13CNMRTRIS(4-METHOXYPHENYL)PHOSPHINE(855-38-9)31PNMRTRIS(4-METHOXYPHENYL)PHOSPHINE(855-38-9)IR1TRIS(4-METHOXYPHENYL)PHOSPHINE(855-38-9)IR2TRIS(4-METHOXYPHENYL)PHOSPHINE(855-38-9)Raman

855-38-9(Tris(4-methoxyphenyl)phosphine)Related Search:

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Phosphine, tris(p-methoxyphenyl)- Phosphorus tri-(p-methoxyphenyl) Tri(p-methoxyphenyl)phosphine Tri-p-anisylphosphine TRIS(P-ANISYL)PHOSPHINE TRIS(4-METHOXYPHENYL)PHOSPHINE TRI(4-METHOXYPHENYL)PHOSPHINE LABOTEST-BB LTBB005439 Tris(4-methoxyphenyl)phosphine,95% Tris(2-methoxyphenyl)-phosphine / Tris(4-methoxyphenyl)-phosphine Tris(p-methoxyphenyl)phosphine,98% TRIS(4-METHOXYPHENYL)PHOSPHINE (TPAP) Phosphine,tris(4-Methoxyphenyl)- Tris(4-Methoxyphenyl)phosphine 95% Tris(4-methoxyphenyl)phosphine,97+% High purity CAS 855-38-9 TRIS(4-METHOXYPHENYL)PHOSPHINE in stock Tris(4-methoxyphenyl)phosphine > Tris(4-methoxyphenyl)phosphine, 95%, for synthesis Tris(p-methoxyphenyl)phosphine 95% TRIS(P-METHOXYP Phosphine,tris(4-METHOXYBENZYL)- (2S)-1-[4-[4-[bis(2-chloroethyl)amino]phenyl]-1-oxobutyl]-2-pyrrolidinecarboxylic acid Tris(4-methoxyphenyL Trianisylphosphine TRIS(P-METHOXYPHENYL)PHOSPHINE tris(4-Methoxyphenyl)phosphane 855-38-9 855-36-9 pCH3OC6H43P C21H21O3P Phosphorus Compounds Catalysis and Inorganic Chemistry Phosphine Ligands Achiral Phosphine Aryl Phosphine organophosphine ligand Ligand Phosphine Ligands Synthetic Organic Chemistry Basic Phosphine LigandsCatalysis and Inorganic Chemistry Catalysis and Inorganic Chemistry Cross-Coupling Phosphine Ligands Phosphorus Compounds