ETHYL 3-BUTENOATE
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ETHYL 3-BUTENOATE 속성
- 녹는점
- 37.22°C (estimate)
- 끓는 점
- 117℃
- 밀도
- 0.904
- 굴절률
- 1.4105
- 인화점
- 31℃
- 물리적 상태
- 액체
- LogP
- 1.540 (est)
안전
HS 번호 | 2916199590 |
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ETHYL 3-BUTENOATE C화학적 특성, 용도, 생산
Synthesis Reference(s)
Journal of the American Chemical Society, 86, p. 4350, 1964 DOI: 10.1021/ja01074a023The Journal of Organic Chemistry, 49, p. 1341, 1984 DOI: 10.1021/jo00182a005
Synthesis
The synthesis of ETHYL 3-BUTENOATE is as follows:step one: At room temperature,to a three-necked flask was added 600 parts of toluene,150 parts of triethylamine, 110 parts of ethanol,100 parts of crotonyl chloride were charged in a constant pressure separatory funnel, under electric stirring, toluene.The mixture of triethylamine and ethanol is mixed well, while heating the mixture to 55 °C, then through the constant pressure funnel control crotonyl chloride uniform dropping 1h, reaction overnight, gas chromatography to detect the progress of the reaction, record the reaction time;step two: The reaction is over. The reaction solution is cooled, the liquid is washed twice with water, dried over anhydrous magnesium sulfate, filtering, removing toluene solvent by rotary evaporation, 3-butenoic acid hexyl ester to give a crude product.
step three: The crude 3-butenyl caproate obtained in step two is in a ratio by weight of crude product: silica gel = 3-4: 1 with 120 mesh silica gel dry packing method, then the volume ratio of petroleum ether - ethyl acetate gradient elution, the eluate obtained by eluting with petroleum ether-ethyl acetate in a volume ratio of 200: 1 was recovered, rotary evaporation of petroleum ether - ethyl acetate. The product, hexyl 3-butenoate, weight and calculate yield.
ETHYL 3-BUTENOATE 준비 용품 및 원자재
원자재
준비 용품
ETHYL 3-BUTENOATE 공급 업체
글로벌( 59)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
---|---|---|---|---|---|
Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 |
sales@capotchem.com | China | 29797 | 60 |
CONIER CHEM AND PHARMA LIMITED | +8618523575427 |
sales@conier.com | China | 49391 | 58 |
Nanjing Triumpharm Co.,Ltd | +86-02586182925 +86-15105172550 |
info@triumpharm.com | China | 129 | 58 |
China National Standard Pharmaceutical Corporation Limited | +8615391658522 |
overseasales@yongstandards.com | China | 11927 | 58 |
Wuhan Topule Biopharmaceutical Co., Ltd | +8618327326525 |
masar@topule.com | China | 8474 | 58 |
LEAPCHEM CO., LTD. | +86-852-30606658 |
market18@leapchem.com | China | 43348 | 58 |
R&D Scientific Inc. | +12266000236 |
sales@rdscientific.com | Canada | 1307 | 58 |
Aladdin Scientific | +1-833-552-7181 |
sales@aladdinsci.com | United States | 57511 | 58 |
Amadis Chemical Company Limited | 571-89925085 |
sales@amadischem.com | China | 131981 | 58 |
Hangzhou Copiore Chemical Co., Ltd. | 0571-56076030 13757145729 |
sales@copiore.com | China | 233 | 58 |
ETHYL 3-BUTENOATE 관련 검색:
에틸 크로톤산 3-(헥사데시닐)다이하이드로-2,5-퓨란다디온 다이하이드로-3-(옥타데세닐)-2,5-퓨란다이올 디하이드로-3-(옥테닐)-2,5-푸란디온 무수데세닐숙신산
TETRADECENYLSUCCINIC ANHYDRIDE
5-Carbethoxy-4,6-dimethyl-2-pyrone
N-DOCOSENYLSUCCINIC ANHYDRIDE
DIBUTYL ITACONATE
CIS-3-HEXENYL CIS-3-HEXENOATE
Ethyl 3-hexenoate
TRIETHYL ACONITATE
1-Dodecenylsuccinic anhydride
4-CARBETHOXY-3-METHYL-2-CYCLOHEXEN-1-ONE
DIETHYL GLUTACONATE
3,6-DIHYDRO-4,6,6-TRIMETHYL-2H-PYRAN-2-ONE
4-CARBETHOXY-2-ETHYL-3-METHYL-2-CYCLOHEXEN-1-ONE
3-BROMO-5-CARBETHOXY-4,6-DIMETHYL-2-PYRONE