SMILAGENIN suppliers
SMILAGENIN
- CAS:
- 126-18-1
- MF:
- C27H44O3
- MW:
- 416.64
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Properties
- Melting point:
- ~185 °C
- alpha
- D25 -69° (c = 0.5 in chloroform)
- Boiling point:
- 474.91°C (rough estimate)
- Density
- 1.0362 (rough estimate)
- refractive index
- 1.4700 (estimate)
- storage temp.
- Store at -20°C
- solubility
- Ethanol: ≥ 10 mg/mL (24.00 mM); DMSO: < 1 mg/mL (insoluble or slightly soluble)
- pka
- 15.14±0.70(Predicted)
Safety Information
- WGK Germany
- 3
- F
- 10
Use
Chromatograph smilagenin on active Al2O3 and elute with *C6H6, then recrystallise it from Me2CO, aqueous EtOH (m 187-188o) or MeOH. The acetate crystallises from MeOH with m 152o and [] D 25 -59.6o, [] 546 25 –68.9o (c 0.25, CHCl3). [Askew J Chem Soc 1399 1936 and 1402 1936, Scheer et al. J Am Chem Soc 77 6411955, Beilstein 19 III/IV 826.]
52 supplier list of "SMILAGENIN"
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