N-(2-AMINOETHYL)-N-ETHYL-M-TOLUIDINE(19248-13-6) ¹³C NMR

Product NameN-(2-AMINOETHYL)-N-ETHYL-M-TOLUIDINE

CAS 19248-13-6

Molecular FormulaC11H18N2

Molecular Weight178.27

InChIInChI=1S/C11H18N2/c1-3-13(8-7-12)11-6-4-5-10(2)9-11/h4-6,9H,3,7-8,12H2,1-2H3

InChIKey FTMVEUXYYDLYFH-UHFFFAOYSA-N

SmilesC(N(CC)C1=CC=CC(C)=C1)CN

Request For Quotation

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-5534          
N-ethyl-N-(m-tolyl)ethylenediamine
C11H18N2            (Mass of molecular ion:    178)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       1.4
      28.0       2.1
      29.0       1.5
      30.0       1.9
      39.0       2.0
      41.0       1.5
      42.0       1.9
      44.0       1.6
      51.0       1.3
      63.0       1.2
      65.0       5.5
      77.0       3.3
      78.0       1.0
      79.0       1.2
      89.0       1.6
      90.0       1.1
      91.0      15.8
      92.0       3.7
      93.0       3.9
     105.0       2.6
     106.0       1.3
     117.0       1.1
     118.0       6.6
     119.0       4.4
     120.0      44.4
     121.0       4.3
     132.0       1.5
     133.0       1.8
     134.0       3.3
     135.0       4.3
     144.0       1.2
     146.0       1.1
     147.0       1.3
     148.0     100.0
     149.0      11.6
     160.0       1.0
     178.0      10.3
     179.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₈ N₂	0.05 ml : 0.5 ml CDCl₃
N-ethyl-N-(m-tolyl)ethylenediamine

    Assign.     Shift(ppm)

      A             7.091
      B             8.54
      C     *1      6.53
      D     *1      6.49
      E             3.363
      F             3.308
      G             2.873
      J             2.295
      K             1.4
      L             1.128

     Hz     ppm     Int.

   2842.16   7.112     97
   2839.60   7.106     46
   2834.96   7.094    129
   2833.13   7.090    118
   2828.74   7.079     37
   2825.68   7.071    114
   2611.94   6.536    335
   2605.35   6.520    135
   2603.03   6.514     73
   2598.27   6.502    142
   2590.82   6.483    134
   1354.74   3.390    117
   1347.78   3.373    337
   1340.70   3.355    340
   1333.62   3.337    126
   1328.98   3.326    215
   1322.27   3.309    411
   1315.55   3.292    239
   1154.79   2.890    311
   1147.95   2.873    520
   1141.24   2.856    270
    917.24   2.296   1000
    551.76   1.381     68
    457.76   1.146    485
    450.81   1.129    907
    443.73   1.111    464

in CDCl3