1-Methylcyclopropanemethanol(2746-14-7) ¹³C NMR

Product Name1-Methylcyclopropanemethanol

CAS 2746-14-7

Molecular FormulaC5H10O

Molecular Weight86.13

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Mass

MS-NW-9933          
(1-methylcyclopropyl)methanol
C5H10O              (Mass of molecular ion:     86)

   Source Temperature: 190 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       1.6
      26.0       2.3
      27.0      17.0
      28.0       8.5
      29.0      23.0
      30.0       8.8
      31.0      14.9
      38.0       2.0
      39.0      19.8
      40.0       7.9
      41.0      29.5
      42.0       3.2
      43.0      13.2
      44.0       5.9
      45.0       3.1
      50.0       2.2
      51.0       2.9
      52.0       1.0
      53.0      11.2
      54.0       3.7
      55.0      24.1
      56.0      46.1
      57.0      49.3
      58.0     100.0
      59.0       4.1
      67.0       6.8
      68.0       8.8
      69.0       2.6
      71.0      11.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₅ H₁₀ O	0.05 ml : 0.5 ml CDCl₃
(1-methylcyclopropyl)methanol

    Assign.     Shift(ppm)

      A             3.367
      B             3.02
      C             1.141
      D     *1      0.396
      E     *1      0.302

     Hz     ppm     Int.

   1345.70   3.368    331
   1206.67   3.020    201
    455.93   1.141   1000
    445.56   1.115     25
    164.55   0.412    125
    160.16   0.401    348
    158.57   0.397    384
    154.54   0.387    186
    125.00   0.313    211
    121.09   0.303    405
    119.38   0.299    345
    114.87   0.288    141

in CDCl3