2-Bromo-3-methylpyridine(3430-17-9) MS

Product Name2-Bromo-3-methylpyridine

CAS 3430-17-9

Molecular FormulaC6H6BrN

Molecular Weight172.02

InChIInChI=1S/C6H6BrN/c1-5-3-2-4-8-6(5)7/h2-4H,1H3

InChIKey PZSISEFPCYMBDL-UHFFFAOYSA-N

SmilesC1(Br)=NC=CC=C1C

Request For Quotation

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-9329          
2-bromo-3-methylpyridine
C6H6BrN             (Mass of molecular ion:    171)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       1.3
      27.0       1.7
      28.0       1.2
      37.0       2.8
      38.0       5.6
      39.0      17.5
      40.0       1.7
      41.0       1.9
      45.5       1.4
      50.0       2.1
      51.0       2.6
      52.0       1.9
      61.0       1.1
      62.0       1.9
      63.0       6.2
      64.0       7.9
      65.0      49.3
      66.0       5.0
      84.5       1.0
      85.5       1.7
      90.0       1.5
      91.0       8.4
      92.0     100.0
      93.0       7.2
     171.0      34.8
     172.0       3.1
     173.0      34.1
     174.0       2.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₆ Br N	0.05 ml : 0.5 ml CDCl₃
2-bromo-3-methylpyridine

    Assign.     Shift(ppm)

      A             8.179
      B             7.510
      C             7.168
      D             2.367

     Hz     ppm     Int.

   3270.51   8.184    118
   3267.09   8.175    117
   3006.71   7.524    131
   3005.74   7.521    129
   2999.27   7.505    143
   2998.29   7.503    139
   2870.61   7.183    138
   2865.84   7.171    141
   2863.16   7.165    129
   2858.40   7.153    119
    945.92   2.367   1000

in CDCl3