D/L-NORVALINOL(4146-04-7) MS
Product NameD/L-NORVALINOL
CAS4146-04-7
Molecular FormulaC5H13NO
Molecular Weight103.16
-
MassMS-NW-7302 DL-2-amino-1-pentanol C5H13NO (Mass of molecular ion: 103)
Source Temperature: 200 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.0 18.0 4.4 27.0 5.1 28.0 7.3 29.0 5.7 30.0 56.2 31.0 3.7 39.0 3.6 41.0 5.0 42.0 14.5 43.0 5.6 44.0 9.0 55.0 7.4 56.0 3.5 57.0 2.4 60.0 28.7 70.0 1.1 72.0 100.0 73.0 5.1 86.0 5.0
90 MHz in CDCl3
-
1H NMR 89.56 MHz C5 H13 N O 0.05 ml : 0.5 ml CDCl3 DL-2-amino-1-pentanol 
Assign. Shift(ppm)
A *1 3.548 B *1 3.261 C 2.94 D 2.78 E 1.38 F 1.26 G 0.93 J(A,B)=-10.7HZ J(A,D)=3.9HZ J(B,D)=7.6HZ
Hz ppm Int.326.81 3.650 102 323.00 3.607 123 316.25 3.532 220 312.38 3.488 234 300.69 3.358 229 297.00 3.317 30 296.50 3.311 31 293.06 3.273 287 290.06 3.239 112 287.44 3.210 34 286.94 3.204 35 286.44 3.199 35 285.88 3.193 34 282.50 3.155 179 263.00 2.937 1000 120.75 1.349 395 88.50 0.989 273 82.88 0.926 572 77.50 0.866 229
in CDCl3
liquid film
