2,4-DINITROPHENYL ACETATE,95%(4232-27-3) ¹H NMR

Product Name2,4-DINITROPHENYL ACETATE,95%

CAS 4232-27-3

Molecular FormulaC8H6N2O6

Molecular Weight226.14

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Mass

MS-IW-3902          
2,4-dinitrophenyl acetate
C8H6N2O6            (Mass of molecular ion:    226)

   Source Temperature: 120 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      15.0       2.2
      28.0       1.4
      30.0       2.4
      38.0       1.3
      42.0       4.2
      43.0     100.0
      44.0       4.2
      50.0       1.1
      51.0       2.6
      53.0       2.8
      61.0       1.1
      62.0       4.3
      63.0       8.1
      64.0       1.6
      74.0       1.1
      79.0       2.0
      91.0       3.0
      92.0       2.0
      93.0       1.2
     107.0       1.9
     154.0       1.4
     168.0       1.4
     184.0       4.6
     226.0       3.8

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₆ N₂ O₆	0.041 g : 0.5 ml CDCl₃
2,4-dinitrophenyl acetate

    Assign.     Shift(ppm)

      A             8.960
      B             8.534
      C             7.502
      D             2.434
     
     J(A,B)=2.7HZ
     J(A,C)=0.4HZ
     J(B,C)=8.9HZ

     Hz     ppm     Int.

   3582.52   8.965    134
   3579.83   8.958    142
   3416.63   8.550    106
   3413.94   8.543    105
   3407.71   8.527    111
   3405.03   8.521    111
   3002.69   7.514    152
   2993.77   7.491    147
    973.02   2.435   1000
    969.12   2.425     27

in CDCl3