1H-Pyrrole-1-carboxylic acid, 2,3-dihydro-, 9H-fluoren-9-ylmethyl ester synthesis

3synthesis methods

Product Name:1H-Pyrrole-1-carboxylic acid, 2,3-dihydro-, 9H-fluoren-9-ylmethyl ester
CAS Number:1359015-06-7
Molecular formula:C19H17NO2
Molecular Weight:291.34

71989-31-6 Synthesis

71989-31-6
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1H-Pyrrole-1-carboxylic acid, 2,3-dihydro-, 9H-fluoren-9-ylmethyl ester

1359015-06-7
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: dicyclohexyl-carbodiimide / ethyl acetate / 24 h / 20 °C / Inert atmosphere
2: bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether / N,N-dimethyl-formamide / 14 h / 20 °C / Inert atmosphere

References:

Garcia-Reynaga, Pablo;Carrillo, Angela K.;Vannieuwenhze, Michael S. [Organic Letters,2012,vol. 14,# 4,p. 1030 - 1033]

1-Pyrrolidinecarboxylic acid, 2-[(phenylthio)carbonyl]-, 9H-fluoren-9-ylmethyl ester, (2S)-

1359014-90-6
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1359015-06-7
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References

103321-52-4
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1359015-06-7
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References