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ChemicalBook CAS DataBase List 2-Nitrobenzoyl chloride

2-Nitrobenzoyl chloride synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium bromide / 12 h / 40 °C
2: triethylamine; bis(trichloromethyl) carbonate / 1,2-dichloro-ethane / 4 h / 60 °C

References:

Anhui Qingyun Pharmaceutical Co., Ltd.;Huang Huan;Huang Qingguo;Zhou Jian CN107652192, 2018, A

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