Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Inquriy
Try our best to find the right business for you.
Messages
Do not miss inquiry messages Please log in to view all inquiry messages.
My chemicalbook

Welcome back!

Structured search
18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 2-(Trimethylsilyl)ethanol

2-(Trimethylsilyl)ethanol synthesis

11synthesis methods
Three methods of preparation have been reported: (a) from the treatment of ethyl bromoacetate with zinc followed by the reaction with chlorotrimethylsilane1 and subsequent reduction of the resultant ethyl trimethylsilylacetate with lithium aluminum hydride2,3 or borane–tetrahydrofuran(eq 1); (b) from the hydroboration/oxidation or oxymercuration/demercuration of vinyltrimethylsilane (eq 2); and (c)most conveniently, by the reaction of the Grignard reagent formed from (chloromethyl)trimethylsilane with paraformaldehyde (eq 3).

Ethyl (trimethylsilyl)acetate

4071-88-9
151 suppliers
$21.00/1g

2-(Trimethylsilyl)ethanol

2916-68-9
313 suppliers
$13.00/5g

-

Yield:2916-68-9 78.1%

Reaction Conditions:

with borane-THF in tetrahydrofuran for 48 h;Ambient temperature;

References:

Rosowsky, Andre;Wright, Joel E. [Journal of Organic Chemistry,1983,vol. 48,# 9,p. 1539 - 1541]

FullText

9-Borabicyclo[3.3.1]nonane, 9-[2-(trimethylsilyl)ethyl]-

72610-05-0
0 suppliers
inquiry

2-(Trimethylsilyl)ethanol

2916-68-9
313 suppliers
$13.00/5g

CIS-1,5-CYCLOOCTANEDIOL

23418-82-8
13 suppliers
$205.00/10g

References
Ethyl trimethylacetate

3938-95-2
150 suppliers
$12.00/25g

2-(Trimethylsilyl)ethanol

2916-68-9
313 suppliers
$13.00/5g

References
Vinyltrimethylsilane

754-05-2
235 suppliers
$11.00/1g

1-(TRIMETHYLSILYL)ETHANOL, 98

13246-39-4
5 suppliers
inquiry

2-(Trimethylsilyl)ethanol

2916-68-9
313 suppliers
$13.00/5g

References
METHYL (TRIMETHYLSILYL)ACETATE

2916-76-9
68 suppliers
$45.00/1g

2-(Trimethylsilyl)ethanol

2916-68-9
313 suppliers
$13.00/5g

References

2-(Trimethylsilyl)ethanol Related Search:

Ethyl acetate Vinyltrimethoxysilane Ethanol Benzyltrimethylammonium chloride allyltrimethylammonium chloride TRIMETHYLSULFOXONIUM CHLORIDE 2-(METHYLDIPHENYLSILYL)ETHANOL 2-(Trimethylsilyl)ethoxymethyl chloride 3-(TRIMETHYLSILYL)-1,2-PROPANEDIOL 2-(TRIMETHYLSILYL)ETHOXYMETHYLTRIPHENYLPHOSPHONIUM CHLORIDE