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Benzenediazonium, 4-(ethoxycarbonyl)-, tetrafluoroborate(1-) synthesis

3synthesis methods
-

Yield:348-06-1 96%

Reaction Conditions:

with tert.-butylnitrite;boron trifluoride diethyl etherate in tetrahydrofuran;dichloromethane at -25 - -20;

References:

Gaud, Vincent;Rougé, Fabien;Gnanou, Yves;Desvergne, Jean-Pierre [Reactive and functional polymers,2012,vol. 72,# 8,p. 521 - 532] Location in patent:experimental part