4-bromonaphthalen-2-ol synthesis
- Product Name:4-bromonaphthalen-2-ol
- CAS Number:5498-31-7
- Molecular formula:C10H7BrO
- Molecular Weight:223.07
134-32-7
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5498-31-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: bromine; acetic acid / 1 h / 70 °C
2: acetic acid; propionic acid; sodium nitrite / 1 h / 5 - 8 °C
3: sodium tetrahydroborate / ethanol / 4 h / 13 - 18 °C
References:
MIRATI THERAPEUTICS, INC.;ARRAY BIOPHARMA, INC.;FISCHER, John, P.;FELL, Jay, Bradford;BLAKE, James, F.;HINKLIN, Ronald, Jay;MEJIA, Macedonio, J.;HICKEN, Erik, James;CHICARELLI, Mark, Joseph;GAUDINO, John, J.;VIGERS, Guy, P.A.;BURGESS, Laurence, E.;MARX, Matthew, Arnold;CHRISTENSEN, James, Gail;LEE, Matthew, Randolf;SAVECHENKOV, Pavel;ZECCA, Henry, J. WO2017/201161, 2017, A1
53846-22-3
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5498-31-7
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$45.00/10mg
20191-76-8
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$15.00/250mg
5498-31-7
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1078-19-9
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$6.00/5g
5498-31-7
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$45.00/10mg
945830-92-2
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5498-31-7
123 suppliers
$45.00/10mg