ChemicalBook CAS DataBase List N,N'-diethyl-N,N'-diphenylthioperoxydicarbamic acid

N,N'-diethyl-N,N'-diphenylthioperoxydicarbamic acid synthesis

5synthesis methods

Product Name:N,N'-diethyl-N,N'-diphenylthioperoxydicarbamic acid
CAS Number:41365-24-6
Molecular formula:C18H20N2S4
Molecular Weight:392.61

75-15-0
233 suppliers
$40.00/100g

103-69-5
250 suppliers
$13.00/100g

N,N'-diethyl-N,N'-diphenylthioperoxydicarbamic acid

41365-24-6
12 suppliers
inquiry

Yield:41365-24-6 98.9%

Reaction Conditions:

with pyridine;dihydrogen peroxide in cyclohexane at 0 - 10; for 6 h;

Steps:

2 Example 2

200mL cyclohexane, 32.1g carbon disulfide, 45.2g N-ethylaniline,0.04g pyridine was added to the 1L flask and stirred; at 010,Slowly add 127.0g of 5% hydrogen peroxide, and finish after 6h; keep warm,TLC followed until the end of the reaction. Suction filtration gave white N,N'-diethyl-N,N'-diphenylthiuram disulfide. The yield is 98.9%,The purity by HPLC was 98.9%.

References:

CN111116439,2020,A Location in patent:Paragraph 0024-0025