O-ethyl-O'-(2-diisopropylaminoethyl)methylphosphonite synthesis
- Product Name:O-ethyl-O'-(2-diisopropylaminoethyl)methylphosphonite
- CAS Number:71840-26-1
- Molecular formula:C11H26NO3P
- Molecular Weight:251.3
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Yield:-
Reaction Conditions:
with triethylamine in dichloromethane at 20; for 1 h;
Steps:
General procedure for microsynthesisof O-alkyl O-2-(N,N-dialkylamino)ethylalkylphosphonates II
General procedure: Alcohol (R2OH, 0.2 mmol), 2-(N,N-dialkylamino)ethanol (0.2 mmol) and triethylamine (0.4 mmol) in CH2Cl2 (200 μL) was added to a solution of alkylphosphonic dichloride (0.2 mmol) in dichloromethane (300 μL) dropwise, while stirring. The reaction mixture was stirred at ambient temperature for an hour. Any precipitate was filtered off and the solution was analyzedusing GC/MS as required.
References:
Saeidian, Hamid;Babri, Mehran;Ramezani, Atefeh;Ashrafi, Davood;Sarabadani, Mansour;Taghi Naseri, Mohammad [European Journal of Mass Spectrometry,2013,vol. 19,# 5,p. 361 - 375]