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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-

4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]- synthesis

6synthesis methods
1-Fluoro-2-nitrobenzene

1493-27-2
503 suppliers
$5.00/10g

4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-

761440-16-8
236 suppliers
$9.00/250mg

-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 20 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol / 6 h
4.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / Cooling
4.2: 16 h / 20 °C

References:

WO2011/140338,2011,A1

isopropyl(2-nitrophenyl)sulfane

70415-85-9
38 suppliers
inquiry

4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-

761440-16-8
236 suppliers
$9.00/250mg

References
1-(isopropylsulfonyl)-2-nitrobenzene

70415-86-0
56 suppliers
$45.00/50mg

4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-

761440-16-8
236 suppliers
$9.00/250mg

References
2-(isopropylthio)aniline

6397-33-7
55 suppliers
$21.00/1g

4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-

761440-16-8
236 suppliers
$9.00/250mg

References
88-73-3 Synthesis
2-Nitrochlorobenzene

88-73-3
8 suppliers
$14.00/25g

4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-

761440-16-8
236 suppliers
$9.00/250mg

References

4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]- Related Search:

2,4,5-Trichloropyrimidine 1-AMINO-2-(ISOPROPYLSULPHONYL)BENZENE 1-broMo-5-fluoro-2-Methyl-4-nitrobenzene 4-(5-isopropoxy-2-Methyl-4-nitrophenyl)pyridine 3-(dimethylamino)-1-(naphthalen-5-yl)propan-1-one 3-benzyl-6-bromo-2-chloroquinoline 5-BROMO-2-(2-METHYL-2H-TETRAZOL-5-YL)-PYRIDINE 4-Bromo-2-nitroaniline 3-benzyl-6-bromo-2-methoxyquinoline CarbaMic acid, N-[3-fluoro-4-[6-(2-Methyl-2H-tetrazol-5-yl)-3-pyridinyl]phenyl]-, phenylMethyl ester