BZ-DMT-DEOXYADENOSINE 2-CLPH DIESTER TRIETHYLAMMONIUM SALT synthesis

1synthesis methods

Product Name:BZ-DMT-DEOXYADENOSINE 2-CLPH DIESTER TRIETHYLAMMONIUM SALT
CAS Number:85381-22-2
Molecular formula:C50H54ClN6O9P
Molecular Weight:949.44

15715-58-9
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$71.00/5g

64325-78-6 Synthesis

N6-Benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine

64325-78-6
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$9.00/250mg

15074-54-1 Synthesis

15074-54-1
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$19.00/1g

BZ-DMT-DEOXYADENOSINE 2-CLPH DIESTER TRIETHYLAMMONIUM SALT

85381-22-2
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Yield:-

Reaction Conditions:

Stage #1: N₆-benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine;2-chlorophenyl dichlorophosphatewith pyridine;1,2,3-triazole in dichloromethane at 0; for 2.5 h;
Stage #2: triethylamine carbonatewith water in dichloromethane;Further stages.;

References:

Yagodkin, Andrey;Azhayev, Alex;Roivainen, Jarkko;Antopolsky, Maxim;Kayushin, Alexei;Korosteleva, Maria;Miroshnikov, Anatoly;Randolph, John;Mackie, Hugh [Nucleosides, nucleotides and nucleic acids,2007,vol. 26,# 5,p. 473 - 497]

BZ-DMT-DEOXYADENOSINE 2-CLPH DIESTER TRIETHYLAMMONIUM SALT Related Search:

4,4'-DIMETHOXYBENZHYDROL 1-TERT-BUTOXY-2-PROPANOL ETHYLENE GLYCOL MONO-TERT-BUTYL ETHER 4-METHOXYBENZHYDROL 6-Benzylaminopurine 5'-O-(4,4'-DIMETHOXYTRITYL)-2'-DEOXYADENOSINE Adenine hydrochloride N-Benzoylaminopurine N6-Benzoyl-5'-O-(4,4'-dimethoxytrityl)-2'-deoxyadenosine 6-(METHYLAMINO)PURINE