ChemicalBook CAS DataBase List ACENAPHTHO[1,2-B]QUINOXALINE

ACENAPHTHO[1,2-B]QUINOXALINE synthesis

6synthesis methods

Product Name:ACENAPHTHO[1,2-B]QUINOXALINE
CAS Number:207-11-4
Molecular formula:C18H10N2
Molecular Weight:254.29

95-54-5 Synthesis

95-54-5
486 suppliers
$9.00/1g

82-86-0 Synthesis

82-86-0
207 suppliers
$10.00/1g

207-11-4
21 suppliers
$28.60/250MG

Yield:207-11-4 98%

Reaction Conditions:

with sulfonated rice husk ash at 20; for 0.0833333 h;Green chemistry;

Steps:

General procedure for the synthesis of quinoxaline derivatives

General procedure: To a mixture of 1,2-diaminobenzene (1 mmol) and 1,2-dicarbonyl compound (1 mmol), RHA-SO₃H (15 mg) was added and the mixture was stirred at room temperature for the appropriate time. The progress of the reaction was monitored by TLC (EtOAc: n-hexane 2:8). After completion of the reaction, ethyl acetate (20 mL) was added to the mixture and the solid catalyst was separated. Then the solvent was evaporated and the resulting solid product was recrystallized from ethanol, producing the pure product in high yields.

References:

Shamsi-Sani, Mahnaz;Shirini, Farhad;Abedini, Masoumeh;Seddighi, Mohadeseh [Research on Chemical Intermediates,2016,vol. 42,# 2,p. 1091 - 1099]

95-54-5 Synthesis

95-54-5
486 suppliers
$9.00/1g

84-11-7 Synthesis