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Benzene, 1-(2,2-dimethoxyethyl)-4-methoxy- synthesis

4synthesis methods
-

Yield:42866-92-2 99%

Reaction Conditions:

with Pyridine-2,6-dicarboxylic acid;iron(II) tetrafluoroborate hexahydrate;[bis(acetoxy)iodo]benzene at 20; for 20 h;Molecular sieve;Inert atmosphere;regioselective reaction;

References:

Chowdhury, Abhishek Dutta;Lahiri, Goutam Kumar [Chemical Communications,2012,vol. 48,# 28,p. 3448 - 3450] Location in patent:supporting information; experimental part