Oxybenzone synthesis
- Product Name:Oxybenzone
- CAS Number:131-57-7
- Molecular formula:C14H12O3
- Molecular Weight:228.24
? with methyl iodide in the presence of sodium hydroxide;
? with a methyl halide;
? with dimethyl sulfate in the presence of sodium hydroxide or alkaline solution.
Yield:131-57-7 94%
Reaction Conditions:
with sodium carbonate at 160 - 170; for 10 h;
Steps:
1 Example 1
300g of 2,4-dihydroxybenzophenone was added to 200g of dimethyl carbonate, and 20g of sodium carbonate was added, mixed and stirred, heated to 160-170°C, refluxed for 10 hours, and the reaction was completed. Distill under reduced pressure at 220-230°C and 1 mmHg to obtain 2-hydroxy-4-methoxybenzophenone with a yield of 94%.
References:
CN112321461, 2021, A Location in patent:Paragraph 0052-0053
131-56-6
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131-57-7
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123-73-9
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131-57-7
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