ChemicalBook CAS DataBase List Tetramethoxymethane

Tetramethoxymethane synthesis

11synthesis methods

Product Name:Tetramethoxymethane
CAS Number:1850-14-2
Molecular formula:C5H12O4
Molecular Weight:136.15

67-56-1 Synthesis

67-56-1
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$7.29/5ml-f

1850-14-2
123 suppliers
$19.00/1g

Yield:1850-14-2 86%

Reaction Conditions:

with vanadia at 180; under 13501.4 Torr; for 0.1 h;Reagent/catalyst;Temperature;

Steps:

9
50 mmol of methanol, 0.02 mmol of V 2 O 5 , 0.0025 mmol of CoOx/C (supporting amount of 0.1% by weight),30 mmol of methanol was added to a 20 mL stainless steel reaction vessel lined with polytetrafluoroethylene, charged with 1.8 MPa of air, heated to 180 ° C, and reacted at this temperature for 0.1 h.The methanol conversion was 80% and the tetramethoxymethane selectivity was 86%.

References:

Dalian Institute of Chemical Physics;Xu Jie;Jia Xiuquan;Ma Jiping;Li Xiaofang;Xu Yongming;Xia Fei;Nie Xin CN107473945, 2017, A Location in patent:Paragraph 0026-0030; 0031-0033; 0034; 0035-0041

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124-41-4 Synthesis