ChemicalBook CAS DataBase List XPhos Pd G1

XPhos Pd G1 synthesis

1synthesis methods

Product Name:XPhos Pd G1
CAS Number:1028206-56-5
Molecular formula:C41H59ClNPPd
Molecular Weight:738.77

XPhos Pd G1 is an insoluble solid that can be prepared by cross-coupling reactions of imidazole derivatives with dioxane.

13078-80-3 Synthesis

13078-80-3
190 suppliers
$10.00/1g

DICHLORO(N,N,N',N'-TETRAMETHYLETHYLENEDIAMINE)PALLADIUM(II)

14267-08-4
107 suppliers
$35.00/100mg

917-54-4
173 suppliers
$52.10/25ml

564483-18-7 Synthesis

564483-18-7
373 suppliers
$5.00/250mg

1028206-56-5
97 suppliers
$56.00/250mg

Yield:1028206-56-5 70%

Reaction Conditions:

in further solvent(s);treatment of palladium compd. with methyllithium in methyl tert-butyl ether at 0°C, treatment with chlorobenzene deriv. and phosphine deriv. in methyl tert-butyl ether at 55°C; recrystn.;

References:

Biscoe, Mark R.;Fors, Brett P.;Buchwald, Stephen L. [Journal of the American Chemical Society,2008,vol. 130,# 21,p. 6686 - 6687]

XPhos Pd G1 Related Search:

SPhos Pd G1, Methyl t-Butyl Ether Adduct RuPhos Palladacycle Gen. 4 t-BuXphos Palladacycle Gen. 4 Xantphos Pd G3 XPhos Pd G4 RuPhos Pd G3