ChemicalBook--->CAS DataBase List--->10147-36-1

10147-36-1

10147-36-1 Structure

10147-36-1 Structure
IdentificationMore
[Name]

1-Propanesulfonyl chloride
[CAS]

10147-36-1
[Synonyms]

1-PROPANESULFONYL CHLORIDE
PROPANE-1-SULFONYL CHLORIDE
PROPANE SULFONYL CHLORIDE
1-Propanesulfonyl Chloride, Pract.
propanesulphonyl chloride
Propane-1-sulfonic acid chloride
[EINECS(EC#)]

233-414-7
[Molecular Formula]

C3H7ClO2S
[MDL Number]

MFCD00007462
[Molecular Weight]

142.6
[MOL File]

10147-36-1.mol
Chemical PropertiesBack Directory
[Melting point ]

-37 °C
[Boiling point ]

78-79 °C/15 mmHg (lit.)
[density ]

1.267 g/mL at 25 °C(lit.)
[vapor density ]

4.9 (vs air)
[refractive index ]

n20/D 1.453(lit.)
[Fp ]

176 °F
[storage temp. ]

Inert atmosphere,2-8°C
[form ]

clear liquid
[color ]

Colorless to Light yellow
[Water Solubility ]

Decomposes in hot water.
[Sensitive ]

Moisture Sensitive
[BRN ]

1747500
[CAS DataBase Reference]

10147-36-1(CAS DataBase Reference)
[NIST Chemistry Reference]

1-Propanesulfonyl chloride(10147-36-1)
[Storage Precautions]

Moisture sensitive
[EPA Substance Registry System]

10147-36-1(EPA Substance)
Safety DataBack Directory
[Hazard Codes ]

C
[Risk Statements ]

R14:Reacts violently with water.
R34:Causes burns.
R36:Irritating to the eyes.
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
[RIDADR ]

UN 3265 8/PG 2
[WGK Germany ]

3
[F ]

10-19-21
[TSCA ]

Yes
[HazardClass ]

8
[PackingGroup ]

III
[HS Code ]

29049090
Hazard InformationBack Directory
[Chemical Properties]

Light yellow liquid
[Uses]

1-Propanesulfonyl chloride was used in synthesis of 1-alkyl-3-methylimidazolium alkanesulfonate ionic liquids.
[Synthesis]

2,4,6-Trichloro-[1,3,5]-triazine (TCT) was added at room temperature to a solution of propane-1-sulfonic acid in acetone dry, followed by NEt3 dropwise. The resulting mixture was irradiated to 80 °C (50 W of MW power) for 20 min in a sealed tube (10 mL pressure-rated reaction vial) in a self-tuning single-mode irradiating synthesizer. The mixture was cooled rapidly to room temperature by passing compressed air through the microwave cavity for 1 min. After cooling to room temperature, the precipitate was filtered off on Celite to afford 1-Propanesulfonyl chloride[1].
1-Propanesulfonyl chloride
[References]

[1] Lidia De Luca, Giampaolo Giacomelli. “An Easy Microwave-Assisted Synthesis of Sulfonamides Directly from Sulfonic Acids.” The Journal of Organic Chemistry 73 10 (2008): 3967–3969.
Spectrum DetailBack Directory
[Spectrum Detail]

1-Propanesulfonyl chloride(10147-36-1)1HNMR
1-Propanesulfonyl chloride(10147-36-1)IR1
Well-known Reagent Company Product InformationBack Directory
[Sigma Aldrich]

10147-36-1(sigmaaldrich)
[TCI AMERICA]

1-Propanesulfonyl Chloride,>98.0%(GC)(T)(10147-36-1)
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