| Identification | Back Directory | [Name]
5,7-DIHYDRO-INDOLO[2,3-B]CARBAZOLE | [CAS]
111296-90-3 | [Synonyms]
5H,7H-indolo[2,3-b]carbazole 5,7-DIHYDRO-INDOLO[2,3-B]CARBAZOLE 1,3-Dihydroindolo[2,3-b ]carbazole Indolo[2,3-b]carbazole, 5,7-dihydro- 5,7-Dihydroindolo[2,3-b]carbazole,96% 5,7-Dihydro-indolo[2,3-b]carbazole
(DHIC) | [Molecular Formula]
C18H12N2 | [MDL Number]
MFCD10687177 | [MOL File]
111296-90-3.mol | [Molecular Weight]
256.31 |
| Chemical Properties | Back Directory | [Melting point ]
348-360℃ | [Boiling point ]
569.8±23.0 °C(Predicted) | [density ]
1.404±0.06 g/cm3 (20 ºC 760 Torr) | [storage temp. ]
Keep in dark place,Inert atmosphere,Room temperature | [form ]
Solid | [pka]
16.70±0.30(Predicted) | [color ]
Pale brown to brown | [InChI]
InChI=1S/C18H12N2/c1-3-7-15-11(5-1)13-9-14-12-6-2-4-8-16(12)20-18(14)10-17(13)19-15/h1-10,19-20H | [InChIKey]
UVHIWKCVGUMHNB-UHFFFAOYSA-N | [SMILES]
N1C2=C(C=CC=C2)C2=C1C=C1NC3=C(C1=C2)C=CC=C3 |
| Hazard Information | Back Directory | [Uses]
5,7-Dihydro-indolo[2,3-b]carbazole could be a useful thermally activated delayed fluorescence (TADF) emitter for making efficient OLEDs. | [Synthesis]
4′,6′-Dinitro-1,1′:3′,1′′-terphenyl 27.5 g (86 mmol) in a 1 L reactor,57.8 g (348 mmol) of triphenylphosphine,300 mL of dichlorobenzene was added and the mixture was stirred under reflux for 3 days. After completion of the reaction, dichlorobenzene was removed, and the residue was separated by column chromatography to obtain 10.8 g 5,7-Dihydro-indolo[2,3-b]carbazole (Yield 49.0%) |
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