| Identification | Back Directory | [Name]
FMoc-α-Me-Lys(Boc)-OH | [CAS]
1202003-49-3 | [Synonyms]
Fmoc-a-Me-Lys(Boc)-OH
Fmoc-α-Me-Lys(Boc)-OH
Fmoc-alpha-Me-Lys(Boc)-OH
Fmoc-α-methyl-L-Lysine(Boc)
Fmoc-alpha-Me-L-Lys(Boc)-OH
FMoc-α-Me-Lys(Boc)-OH USP/EP/BP
N6-Boc-N2-Fmoc-alfa-Me--L-Lys-OH
N6-Boc-N2-Fmoc-2-methyl-L-Lysine
(S)-Na-Fmoc-Nw-Boc-A-Methyllysine
(S)-NΑ-FMOC-NΩ-BOC-Α-METHYLLYSINE
(S)-Na-Fmoc-NW-Boc-α-Methyllysine
(S)-N-ALPHA-FMOC-N-EPSILON-BOC-ALPHA-METHYLLYSINE
(S)-N-ALPHA-FMOC-N-EPSILON-BOC-ALPHA-METHYLLYSINE, >97%
(9H-Fluoren-9-yl)MethOxy]Carbonyl Alpha-Methyl-Lys(Boc)-OH
N-α-(9-Fluorenylmethoxycarbonyl)-N-ε-(t-butoxycarbonyl)-α-methyl-L-lysine
N6-[(1,1-Dimethylethoxy)carbonyl]-N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-2-methyl-L-lysine
L-Lysine, N6-[(1,1-dimethylethoxy)carbonyl]-N2-[(9H-fluoren-9-ylmethoxy)carbonyl]-2-methyl-
(S)-2-((((9H-Fluoren-9-yl)methoxy)carbonyl)amino)-6-((tert-butoxycarbonyl)amino)-2-methylhexanoic acid
(2S)-6-{[(tert-butoxy)carbonyl]amino}-2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-2-methylhexanoic acid | [Molecular Formula]
C27H34N2O6 | [MDL Number]
MFCD17019258 | [MOL File]
1202003-49-3.mol | [Molecular Weight]
482.57 |
| Chemical Properties | Back Directory | [Boiling point ]
687.9±55.0 °C(Predicted) | [density ]
1.196±0.06 g/cm3(Predicted) | [storage temp. ]
Sealed in dry,2-8°C | [form ]
powder | [pka]
3.92±0.41(Predicted) | [color ]
white |
| Hazard Information | Back Directory | [Chemical Properties]
White to off-white powder. | [Uses]
(S)-2-((((9H-Fluoren-9-yl)methoxy)carbonyl)amino)-6-((tert-butoxycarbonyl)amino)-2-methylhexanoic acid is a reagent in the preparation/biological evaluation of a vapreotide analogs containing (S)-α-methyl-lysine. | [Synthesis]
Benzyl (2R,3S)-(?)-6-oxo-2,3-diphenyl-4-morpholinecarboxylate (4) was successively alkylated with methyl iodide and 1,4-diiodobutane using a base. In each alkylation step anti-alkylated product formed exclusively. The iodo group was displaced with azide, which served as a precursor for the side-chain amino function. Catalytic hydrogenation with concomitant cleavage of the chiral auxiliary afforded (L)-α-Me-Lys-OH (9) in a total of four steps in good yield. (L)-Fmoc-α-Me-Lys(Boc)-OH (16) was obtained from 9 via regioselective benzyloxycarbonylation. Alternately, (L)-Fmoc-α-Me-Lys(Boc)-OH (16) was obtained via Staudinger reduction of azide (8) in a total of six steps in good yield. |
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