1502-06-3

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1502-06-3 Structure

Identification	Back Directory
[Name] CYCLODECANONE
[CAS] 1502-06-3
[Synonyms] NSC 90293 CYCLODECANONE Ketocyclodecane CYCLODECAN-1-ONE Cyclodecanone,97% Cyclodecanone 97% CYCLODECANONE CRYSTALLINE N-(6-amino-1-methyl-2,4-dioxo-5-pyrimidinyl)formamide
[EINECS(EC#)] 216-119-8
[Molecular Formula] C10H18O
[MDL Number] MFCD00003713
[MOL File] 1502-06-3.mol
[Molecular Weight] 154.25

Chemical Properties	Back Directory
[Melting point ] 21-24 °C(lit.)
[Boiling point ] 106-107 °C12 mm Hg(lit.)
[density ] 0.958 g/mL at 25 °C(lit.)
[refractive index ] n20/D 1.482(lit.)
[Fp ] 180 °F
[storage temp. ] 2-8°C
[solubility ] Chloroform (Slightly), Methanol (Slightly)
[form ] Colourless Oil to Semi-Solid
[BRN ] 1617127
[LogP] 2.929 (est)

Hazard Information	Back Directory
[Chemical Properties] White solid or colorless liquid
[Synthesis Reference(s)] Journal of the American Chemical Society, 86, p. 3068, 1964 DOI: 10.1021/ja01069a019 Organic Syntheses, Coll. Vol. 4, p. 218, 1963 Synthetic Communications, 9, p. 437, 1979 DOI: 10.1080/00397917908064174
[Purification Methods] Purify the ketone via the semicarbazone (m 205-207o, from EtOH) and distil it through an efficient column. It sublimes in a vacuum. The oxime has m 80o, from MeOH or by sublimation in a high vacuum. [Cope et al. Org Synth Coll Vol IV 218 1963, Prelog et al. Helv Chim Acta 30 1746 1947, Ruzicka et al. Helv Chim Acta 11 675 1930, Beilstein 7 III 134, 7 IV 76.]

Spectrum Detail	Back Directory
[Spectrum Detail] CYCLODECANONE(1502-06-3)MS CYCLODECANONE(1502-06-3)¹HNMR CYCLODECANONE(1502-06-3)¹³CNMR CYCLODECANONE(1502-06-3)IR1 CYCLODECANONE(1502-06-3)Raman

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