| Identification | Back Directory | [Name]
Dicyclohexylborane | [CAS]
1568-65-6 | [Synonyms]
icyclohexylboron
Dicyclohexylborane
Borane, dicyclohexyl- | [Molecular Formula]
C12H23B | [MDL Number]
MFCD00015771 | [MOL File]
1568-65-6.mol | [Molecular Weight]
178.12 |
| Chemical Properties | Back Directory | [Melting point ]
103-105 °C | [Boiling point ]
263.7±23.0 °C(Predicted) | [solubility ]
Soluble in THF, diethyl ether, dichloromethane, and pentane. |
| Hazard Information | Back Directory | [Uses]
Dicyclohexylborane is a reducing reagent such as in the synthesis of chlorosulfolipid products such as deschloromytilipin A. | [Synthesis Reference(s)]
Journal of the American Chemical Society, 95, p. 6876, 1973 DOI: 10.1021/ja00801a081 | [Reactivity Profile]
Dicyclohexylborane is a reagent for the reduction of ketones and α,β-unsaturated ketones; it is used for the hydroboration of alkynes, alkenes, and allenes.
| [Synthesis]
Dicyclohexylborane is a stable white solid available via the hydroboration of cyclohexene with either Borane-Tetrahydrofuran or Borane-Dimethyl Sulfide. Recently, dicyclohexylborane has been prepared via the hydroboration of cyclohexene with borane-1,4-thioxane.
| [Precautions]
Dicyclohexylborane must be used immediately upon generation or stored as a solid under dry nitrogen. Use in a fume hood.
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parabiochem
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AFINE CHEMICALS LIMITED
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