| Identification | Back Directory | [Name]
4-NITROANILINE HYDROCHLORIDE | [CAS]
15873-51-5 | [Synonyms]
Einecs 239-997-4
4-nitroanilinium chloride
1-Amino-4-nitrobenzeneHCl
P-NITRANILINE HYDROCHLORIDE
P-NITROANILINE HYDROCHLORIDE
4-NITROANILINE HYDROCHLORIDE
4-NITROPHENYLAMINE HYDROCHLORIDE
4-nitro-benzenaminmonohydrochloride
1-AMINO-4-NITROBENZENE HYDROCHLORIDE
Benzenamine, 4-nitro-, monohydrochloride
Benzenamine, 4-nitro-, hydrochloride (1:1) | [EINECS(EC#)]
239-997-4 | [Molecular Formula]
C6H7ClN2O2 | [MDL Number]
MFCD00054338 | [MOL File]
15873-51-5.mol | [Molecular Weight]
174.58 |
| Hazard Information | Back Directory | [Synthesis]
GENERAL METHOD: To a 0.6 mL THF solution of the nitro compound (2 mmol) was added Fe(acac)3 (10 mol%, 70 mg) and TMDS (1.5 eq., equivalent to tris-Si-H, 0.53 mL). The reaction mixture was heated under constant stirring for 24 hours (unless otherwise stated). Upon completion of the reaction, the reaction mixture was diluted with a minimal amount of Et2O. Subsequently, a solution of Et2O with HCl (2 equivalents) was added dropwise. After precipitate generation was observed, stirring was continued for 5 minutes and then filtered. The precipitate was washed several times with Et2O and dried to give 4-nitroaniline hydrochloride. | [References]
[1] Tetrahedron, 2011, vol. 67, # 10, p. 1971 - 1976
[2] Journal of Organic Chemistry, 2009, vol. 74, # 18, p. 6960 - 6964 |
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