| Identification | Back Directory | [Name]
2-Amino-N-methyl-acetamide | [CAS]
22356-89-4 | [Synonyms]
Einecs 244-934-9
Glycine MethylaMide
Acetamide, 2-amino-N-methyl-
Aminoacetic acid methyl amide
N~1~-methylglycinamide hydrochloride
N~1~-methylglycinamide(SALTDATA: HCl) | [EINECS(EC#)]
244-934-9 | [Molecular Formula]
C3H8N2O | [MDL Number]
MFCD06375945 | [MOL File]
22356-89-4.mol | [Molecular Weight]
88.11 |
| Chemical Properties | Back Directory | [Boiling point ]
275.6±23.0 °C(Predicted) | [density ]
1.005±0.06 g/cm3(Predicted) | [storage temp. ]
Keep in dark place,Sealed in dry,Room Temperature | [pka]
15.37±0.46(Predicted) |
| Hazard Information | Back Directory | [Synthesis]
The general procedure for the synthesis of 2-amino-N-methylacetamide from compound 12a (CAS:21855-72-1) was as follows: 10% Pd/C catalyst was added to a methanol (10 mL) solution of compound 12a (170 mg, 0.77 mmol). The hydrogenation reaction was carried out at room temperature and atmospheric pressure for 3 hours. Upon completion of the reaction, the catalyst was removed by diatomaceous earth filtration and the resulting clarified solution was dried to give 2-amino-N-methylacetamide as an oily product. The yield was 97%. The molecular formula is C3H9N2O. | [References]
[1] Patent: WO2006/103463, 2006, A1. Location in patent: Page/Page column 15; Figure 3
[2] Bioorganic and Medicinal Chemistry, 2011, vol. 19, # 3, p. 1285 - 1297
[3] Journal of Organic Chemistry, 1977, vol. 42, # 12, p. 2105 - 2108
[4] Synthesis, 1977, p. 478 - 480 |
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| Company Name: |
Energy Chemical
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021-021-58432009 400-005-6266 |
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http://www.energy-chemical.com |
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